-40%

USED 12 Liter Distillation Unit with NO NEED TO RE-DISTILL !

$ 664.75

Availability: 100 in stock

Description

How to Improve the Purity of Your Distillations & Run Faster with a 12 Liter (!) Unit
USED 12 Liter Distillation Unit with Purification Column, Mantle, Addition Funnel
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Shipping is to an easily verified laboratory address only.
If you increase the purity of your distillations by re-distilling this unit could save you lots of time.  The purification column above the round bottom flask improves the purity of your distillations automatically WITHOUT the need to re-distill saving you LOTS of time.  It does this using a series of glass  plates inside the column, if you want to read more about  how it does this go to the Wikipedia and look up fractionating column.   OR go to You Tube and watch the video from the American Institute of Chemical Engineers, "Distillation Basics - How a Distillation Column Works."   If you do lots of re-distilling this purification column is going to be a huge improvement for most distillations.
If you do  lots of distillations and you have to shut down to re-load the round bottom flask, the addition funnel will save you  lots of time because you can add solvent continuously without removing the round bottom flask from the heat.  The pressure equalizing tube is a great feature because it means the solvent will run smoothly into the flask  instead of the uneven flow of soda out of a soda bottle.
The vacuum adapter allows you to attach a vacuum pump (not included) to complete your distillations using less heat at a lower temperature, recoveries may be lower.
The tubing  is a very soft plastic that is easy to put on the tubulations without breaking them.
The glassware is used and it is in excellent condition.
--- 12 liter round bottom flask, 50/50 ground glass joint
--- 1000 ml Ace Glass addition funnel, pressure equalizing, glass stopcock, 24/40 ground glass joints on both ends
--- Oldershaw column, Lab Glass, 5 plates, vacuum jacketed, bellows, silvered, 29/42 ground glass joints both ends
--- Graham Condenser, 19.5 inch long jacket, 24/40 ground glass  joint on both ends
--- 250 ml collection flask, Pyrex, 24/40 ground glass joint
--- adapters, 50/50 to 29/42, 29/42 to 24/40 (2), 29/42 x 2 & 10/30, 29/42 x 3
--- vacuum adapter, 24/40 x 2
--- YES!  the tubing shown  is included
--- YES!  the colored plastic ground glass joint connectors are included
--- YES!  the glass stoppers shown are included
--- YES!  the power cords shown are included
--- YES!  the cork RBF stand is included
--- not included: lab stands, three finger clamps, wood blocks underneath the RBF
--- possible concerns: the heating  mantle is designed to be held in a large round ring, the cork RBF stand by itself does not raise it quite high enough, the adapter that brings the 29/42 ground glass  joint down to 24/40 so that the addition funnel will fit appears to be stuck in place, but the adapter needs to be in place anyway for the addition funnel to fit properly
--- the unit will ship in 3 boxes for added safety
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What do I need to run this item that is NOT included?
You will need to assemble and install this item.
You will need a transformer to control the temperature of the heating mantle, and you might need two.
You will need a source of cold water for the condenser.
You will want to use a lab scaffold to safely support the unit, several are for sale from this vendor.
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